反应详情

温度

80 °C

To 5-methoxy-2,3,3-trimethyl-3H-indole (1.9 g) was added iodoethane (5 ml) and 1,2-dichlorobenzene (10 ml). The mixture was heated to 80° C. for 4 hours after which time the mixture was allowed to cool and the precipitate removed by filtration and washed sequentially with dichlorobenzene and diethyl ether. Drying in a vacuum oven gave the product (3 g).

1. temperatureto cool
2. customthe precipitate removed by filtration
3. washwashed sequentially with dichlorobenzene and diethyl ether
4. customDrying in a vacuum oven