反应详情

The titled compound was prepared by the method of Example 2, step (f) using the product from example 6, step (e) (75 mg). The reaction mixture was poured into water and acidified with conc. HCl. The suspended solid was removed by filtration, dried in air and recrystallized from acetonitrile to give a yellow solid (37 mg).

1. customThe suspended solid was removed by filtration
2. customdried in air
3. customrecrystallized from acetonitrile