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HRID2105337

反应详情

EQUATION

反应方程式

HRID 2105337 的结构方程式

REACTANTS

反应物

4
结构：CCCCP(CCCC)CCCC
HCID13831

Tributylphosphine

C12H27P

结构：O=C(N=NC(=O)N1CCCCC1)N1CCCCC1
HCID73042

1,1′-(1,2-Diazenediyl)bis[1-(1-piperidinyl)methanone]

C12H20N4O2

结构：CC(C)N1CCC(O)CC1
HCID79681

1-Isopropylpiperidin-4-ol

C8H17NO

结构：C[C@@H]1CNC(=O)c2cc3cc(O)ccc3n21
HCID68465924

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)N1CCC(Oc2ccc3c(c2)cc2n3[C@H](C)CNC2=O)CC1
HCID16679612

未命名化合物

收率 22%

PROCEDURE

实验过程

The title compound was synthesized in analogy to example 1, from (R)-8-hydroxy-4-methyl-3,4-dihydro-2H-pyrazino[1,2-a]indol-1-one, 1-isopropyl-piperidin-4-ol (commercially available), tributylphosphine and 1,1′-(azodicarbonyl)dipiperidine, to give the desired product as a colorless gum (22%).