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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2105439Generated: October 29, 2026

HCID 68424210, compound → HCID 86612932, compound

https://huagongshe.com/reaction/2105439

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68424210HCID 68424210—
CatalystHCID 178418406HCID 178418406—
SolventDichloromethaneHCID 6344—
ProductHCID 86612932HCID 8661293274%

Reaction Steps

The suspension of 0.3 g (1.2 mmol) (5-benzyloxy-1H-pyrrolo[2,3-b]pyridin-2-yl)-methanol and 0.82 g (9.4 mmol) manganese dioxide in 15 ml dichloromethane was stirred 3 h at room temperature. After filtration over dicalite speed plus® (Aldrich) the solvent was evaporated to give 0.22 g (74%) of the desired compound as a light brown solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07579351B2
Source datasetuspto-grants-2009_08
ORD IDord-7474e6cc68b5494ba823d3ab7d3dd892
Source noteuspto-grants-2009_08