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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2105771Generated: November 2, 2026

Phenethylamine → HCID 58998972, compound

https://huagongshe.com/reaction/2105771

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPhenethylamineHCID 1001—
ReactantMethyl acetoacetateHCID 7757—
Reactant3,3,3-TrifluoropropylamineHCID 10001—
Reactant2-Bromo-1-(3,5-difluorophenyl)ethanoneHCID 2778331—
ProductHCID 58998972HCID 58998972—

Reaction Steps

The title compound was synthesized in analogy to Example 68, using 3-oxo-butyric acid methyl ester as compound of formula R, 2-bromo-1-(3,5-difluoro-phenyl)-ethanone as compound of formula S, phenethylamine as R3—(CH2)m—NH2 and 3,3,3-trifluoro-N-propylamine as R1R2NH, MS (ISP) 437.2 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07579369B2
Source datasetuspto-grants-2009_08
ORD IDord-36363c4a3b90462dac21dfd298188018
Source noteuspto-grants-2009_08