HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromopropane → HCID 68815501, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromopropane | HCID 6358 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 68813278 | HCID 68813278 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 68815501 | HCID 68815501 | — |
Reaction Steps
Preparation according to Example 2: 4-[2-fluoro-3-(trifluoromethyl)phenyl]piperidin-4-ol (0.02 g, 0.076 mmol), acetonitrile (2 ml), potassium carbonate (0.02 g, 0.14 mmol), 2-bromopropane (0.008 ml, 0.082 mmol). MS m/z (relative intensity, 70 eV) 305 (M+, 5), 290 (79), 191 (30), 163 (18), 56 (bp).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07579474B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-7522129691f641a1a9774215cc082fe2 |
| Source note | uspto-grants-2009_08 |