HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl bromide → HCID 68815496, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl bromide | HCID 8002 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 17895683 | HCID 17895683 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 68815496 | HCID 68815496 | — |
Reaction Steps
Preparation according to Example 2: 4-(2,3-dichlorophenyl)piperidine (0.02 g, 0.081 mmol), acetonitrile (2 ml), potassium carbonate (0.02 g, 0.14 mmol), bromobutane (0.009 ml, 0.082 mmol). MS m/z (relative intensity, 70 eV) 303 (M+, 2), 302 (M+, 4), 260 (65), 258 (bp), 242 (18), 240 (27).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07579474B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-2296f46551fa419594f17f0880eb300c |
| Source note | uspto-grants-2009_08 |