HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 68814252, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1,1,1-Trifluoro-3-iodopropane | HCID 156165 | — |
| Reactant | HCID 17895683 | HCID 17895683 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 68814252 | HCID 68814252 | — |
Reaction Steps
Preparation according to Example 2: 4-(2,3-dichlorophenyl)piperidine (0.02 g, 0.081 mmol), acetonitrile (2 ml), potassium carbonate (0.02 g, 0.14 mmol), 1,1,1-trifluoro-3-iodopropane (0.010 ml, 0.082 mmol). MS m/z (relative intensity, 70 eV) 343 (M+, 10), 341 (M+, 15), 260 (52), 258 (82), 152 (54), 42 (bp).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07579474B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-8e464007f66545e2b5c8fcc9a4b1f9a7 |
| Source note | uspto-grants-2009_08 |