HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 23149867, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 68815751 | HCID 68815751 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 23149867 | HCID 23149867 | — |
Reaction Steps
According to Preparation 2: Tert-butyl 4-[4-methyl-3-(trifluoro-methyl)phenyl]-4-hydroxypiperidine-1-carboxylate (5.5 g, 15.3 mmol, methylen chloride (30 ml), trifluoroacetic acid (4.5 ml). Yield: 1.97 g. MS m/z (rel. intensity, 70 eV) 259 (M+, 14), 241 (84), 240 (43), 187 (19), 56 (bp).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07579474B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-69926036db2844adac393e3324bdd5d4 |
| Source note | uspto-grants-2009_08 |