HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 57810586, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Bromopinacolone | HCID 21642 | — |
| Reactant | HCID 57810544 | HCID 57810544 | — |
| Product | HCID 57810586 | HCID 57810586 | 94% |
Reaction Steps
5-[1-Ethyl-1-(4-hydroxy-3-methyl-phenyl)-propyl]-3-methyl-benzofuran-2-carboxylic acid ethyl ester (4.04 g, 10.6 mmol) and 1-bromopinacolone (2.66 g, 14.9 mmol) and K2CO3 (2.91 g, 21.2 mmol) are reacted analogous to Example 1E to give the title compound as a pale yellow oil (4.77 g, 94%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07579488B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-830d38c09a8b4dd2bf03bf2dcea3252e |
| Source note | uspto-grants-2009_08 |