HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dichloroethane → HCID 11784862, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dichloroethane | HCID 11 | — |
| Reactant | Dimethylamine, hydrochloride | HCID 10473 | — |
| Reactant | HCID 11328417 | HCID 11328417 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Product | HCID 11784862 | HCID 11784862 | 37.2% |
Reaction Steps
5-{1-[4-(3,3-Dimethyl-2-oxo-butoxy)-3-methyl-phenyl]-1-ethyl-propyl}-3-methyl-benzofuran-2-carboxylic acid (520 mg, 1.154 mmol), DMAP (422 mg, 3.46 mmol), EDC (332 mg, 1.73 mmol), and dimethyl amine hydrochloride (141 mg, 1.73 mmol) are reacted analogous to Example 1, step I to give the title product (205 mg, 37%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07579488B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-fc0dc5ae65ca491aa04a8edcc5a7bd6b |
| Source note | uspto-grants-2009_08 |