HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl bromoacetate → HCID 57810562, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1,8-Diazabicyclo(5.4.0)undec-7-ene | HCID 81184 | — |
| Reactant | 5-(Benzyloxy)-2-hydroxybenzaldehyde | HCID 878362 | — |
| Product | HCID 57810562 | HCID 57810562 | 84% |
Reaction Steps
5-Benzyloxy-2-hydroxy-benzaldehyde ((21.5 g, 94.2 mmol) and ethyl bromoacetate (17.3 g, 103.6 mmol) and K2CO3 (19.5 g, 141.3 mmol) and DBU (14.3 g, 94.2 mmol) are reacted analogous to Example 18-A to give the title compound (23.5 g, 84%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07579488B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-02df3d77817646a0a9ed2620b43b5297 |
| Source note | uspto-grants-2009_08 |