HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 57810536, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Bromopinacolone | HCID 21642 | — |
| Reactant | HCID 57810538 | HCID 57810538 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 57810536 | HCID 57810536 | 90% |
Reaction Steps
6-[1-Ethyl-1-(4-hydroxy-3-methyl-phenyl)-propyl]-benzofuran-2-carboxylic acid ethyl ester (1.58 g, 4.31 mmol) and 1-bromopinacolone (1.16 g, 6.47 mmol) and K2CO3 (1.78 g, 12.9 mmol) in acetone (50 mL) are reacted analogous to Example 30-D to give the title compound (1.80 g, 90%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07579488B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-d7c62f38182a4a11860d2d1c03b177fb |
| Source note | uspto-grants-2009_08 |