HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 57810576, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 68813362 | HCID 68813362 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 57810576 | HCID 57810576 | 68.1% |
Reaction Steps
5-{1-[4-(3,3-Dimethyl-2-oxo-butoxy)-3-ethyl-phenyl]-1-ethyl-propyl}-7-methyl-benzofuran-2-carboxylic acid ethyl ester (1.87 g, 3.91 mmol) in THF (50 mL) is reacted with NaBH4 (0.45 g, 11.7 mmol) analogous to Example 22 to obtain the title compound (1.28 g, 68%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07579488B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-28b958c0172741e881d9ae896fae3396 |
| Source note | uspto-grants-2009_08 |