HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → HCID 15016247, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | 2-(4-Chlorophenyl)hydrazine-1-carbothioamide | HCID 2763665 | — |
| Product | HCID 15016247 | HCID 15016247 | — |
Reaction Steps
Twelve g of 1-(4-chlorophenyl)thiosemicarbazide was suspended in 60 ml of 95% formic acid, and the mixture was stirred under reflux for 24 hours. The mixture was then cooled, and the product precipitated. It was collected and washed with cold denatured ethanol, and was dried to obtain 6.1 g of the desired intermediate, m.p. 222°-224°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04931083 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-65c86ade16d14ffd8c61b1d58842ddc7 |
| Source note | uspto-grants-1990_06 |