HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 14268788, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Ethyl 2-bromopropionate | HCID 79040 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 178517974 | HCID 178517974 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 14268788 | HCID 14268788 | 92.6% |
Reaction Steps
The process was carried out essentially according to that of Example 2 above, starting with 1.2 g of sodium, 30 ml of methanol, 10 g of 1-(2-chlorophenyl)-3-hydroxy-1,2,4-1H-triazole and 9.3 g of ethyl 2-bromopropionate. The solvent was 100 ml of dimethylsulfoxide. The product obtained was 14 g of the desired product, an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04931083 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-8dbed60f8879495d9a34f6a52b772c60 |
| Source note | uspto-grants-1990_06 |