HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 15016259, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Ethyl 2-bromopropionate | HCID 79040 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 178517961 | HCID 178517961 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 15016259 | HCID 15016259 | 77.4% |
Reaction Steps
The process was carried out as described in Example 3, starting with 2.8 g of sodium, 50 ml of ethanol, 75 ml of dimethylsulfoxide, 29 g of 1-(3-bromophenyl)-3-hydroxy-1,2,4-1H-triazole and 21.9 g of ethyl 2-bromopropionate. The yield was 31.8 g of the desired product, m.p. 83°-85°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04931083 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-f5fb8ea5271b4e3dacde34b057c6e5ae |
| Source note | uspto-grants-1990_06 |