Hydrochloric Acid → HCID 15016244, compound

HRID 2106583Notes

Reaction equation

HRID 2106583 reaction equation
C([O:3][C:4]([CH:6]([O:8][C:9]1[N:13]=[CH:12][N:11]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[N:10]=1)[CH3:7])=[O:5])C.[OH-].[K+].Cl>C(O)C>[C:4]([CH:6]([O:8][C:9]1[N:13]=[CH:12][N:11]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[N:10]=1)[CH3:7])([OH:5])=[O:3]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 14797Potassium HydroxideHCID 14268787HCID 14268787, compound

Product 1

HCID 15016244HCID 15016244, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A 2.5 g portion of the compound of Example 1 and 2.2 g of potassium hydroxide were added to 50 ml of ethanol, and the mixture was refluxed for 3 hours. It was then poured into ice-water and the mixture was made acid with concentrated hydrochloric acid. The solid was collected and crystallized from ethanol to obtain 0.9 g of the desired product, m.p. 140°-142°.

Workup

  1. temperaturethe mixture was refluxed for 3 hours
  2. customThe solid was collected
  3. customcrystallized from ethanol

Sources & evidence

ORD record
ord-0f3a62fca0a3405388cfa02db939c27f
Source dataset
uspto-grants-1990_06
Patent number
US04931083

Reaction notes

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