Methylamine → HCID 15016282, compound

Participants

Reaction Steps

A 2.5 g portion of the compound of Example 1 was combined with 10 ml of 40% aqueous methylamine and 20 ml of dimethylformamide at room temperature, and the mixture was allowed to stand for 2 days. It was then poured into ice-water, and the solid was collected and air-dried to obtain 0.4 g of the desired product, m.p. 134°-135°.

Provenance & Evidence