HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → HCID 15016284, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | HCID 15016262 | HCID 15016262 | — |
| Product | HCID 15016284 | HCID 15016284 | 56.2% |
Reaction Steps
The process was carried out as was Example 45, starting with 5 g of the compound of Example 24, 4 g of carbonyldiimidazole and 1.2 g of ammonium hydroxide. The yield was 2.8 g of the desired product, m.p. 147°-149°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04931083 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-c8a1e1f5d35c4796b9f3626e994fa199 |
| Source note | uspto-grants-1990_06 |