HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 15016285, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | HCID 15016263 | HCID 15016263 | — |
| Product | HCID 15016285 | HCID 15016285 | 66.6% |
Reaction Steps
The process was carried out as was Example 45, starting with 3 g of the compound of Example 25, 2.7 g of carbonyldiimidazole and 3.6 ml of 40% aqueous dimethylamine. The product was recrystallized from toluene to obtain 2.2 g of desired product, m.p. 136°-139°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04931083 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-e351cb6b7bb04e08b77b2ea9cb3f0145 |
| Source note | uspto-grants-1990_06 |