HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 15016286, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | HCID 15016263 | HCID 15016263 | — |
| Product | HCID 15016286 | HCID 15016286 | 73.1% |
Reaction Steps
The process was carried out as was Example 45, starting with 3 g of the compound of Example 25, 2.7 g of carbonyldiimidazole, and 3 ml of 40% aqueous methylamine. The product was recrystallized from toluene to obtain 2.3 g of the desired product, m.p. 120°-122°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04931083 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-6a834459e3bd4792a6966ae6a339b383 |
| Source note | uspto-grants-1990_06 |