HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 15016245, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 15016244 | HCID 15016244 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 15016245 | HCID 15016245 | — |
Reaction Steps
A 22.8 g portion of the compound of Example 22 was suspended in 150 ml of toluene, and 49 ml of thionyl chloride was added. The mixture was heated under reflux for 2 hours, and was then cooled and evaporated under vacuum. One hundred ml of additional toluene was added and was removed under vacuum, and the residue was recrystallized from toluene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04931083 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-5726c282ed82482b9ffb9b5e4fab87e0 |
| Source note | uspto-grants-1990_06 |