HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → HCID 15016296, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | Cyclopropylamine | HCID 69828 | — |
| Reactant | HCID 15016275 | HCID 15016275 | — |
| Product | HCID 15016296 | HCID 15016296 | 77% |
Reaction Steps
The process was carried out according to Example 59, starting with 3 g of the compound of Example 37, 2.4 g of carbonyldiimidazole and 1.1 g of cyclopropylamine. product was recrystallized from ethanol to obtain 2.6 g of the desired product, m.p. 170°-172°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04931083 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-5f6abddefcdb4bae89eed97dbfebb628 |
| Source note | uspto-grants-1990_06 |