Ammonium Hydroxide → HCID 15016301, compound

HRID 2106619Notes

Reaction equation

HRID 2106619 reaction equation
[C:1]([CH:4]([O:6][C:7]1[N:11]=[CH:10][N:9]([C:12]2[CH:17]=[CH:16][C:15]([C:18]([F:21])([F:20])[F:19])=[CH:14][CH:13]=2)[N:8]=1)[CH3:5])(O)=[O:2].[OH-].[NH4+:23]>>[NH2:23][C:1]([CH:4]([O:6][C:7]1[N:11]=[CH:10][N:9]([C:12]2[CH:17]=[CH:16][C:15]([C:18]([F:21])([F:20])[F:19])=[CH:14][CH:13]=2)[N:8]=1)[CH3:5])=[O:2]

Participants

3

Reactant 2

HCID 14923Ammonium HydroxideHCID 15016300HCID 15016300, compound

Product 1

HCID 15016301HCID 15016301, compound

Procedure

Three g of the product of Example 65 was reacted with 0.7 g of 35% ammonium hydroxide, substantially as shown in Example 60, to obtain 2 g of the desired product, m.p. 178°-180°.

Sources & evidence

ORD record
ord-1ea41cc451664d61aabb32c7086d4345
Source dataset
uspto-grants-1990_06
Patent number
US04931083

Reaction notes

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