Methylamine → HCID 15016304, compound

HRID 2106622Notes

Reaction equation

HRID 2106622 reaction equation
[C:1]([CH:4]([O:6][C:7]1[N:11]=[CH:10][N:9]([C:12]2[CH:17]=[CH:16][C:15]([C:18]([F:21])([F:20])[F:19])=[CH:14][CH:13]=2)[N:8]=1)[CH3:5])([OH:3])=O.[CH3:22][NH2:23]>>[CH3:22][NH:23][C:1]([CH:4]([O:6][C:7]1[N:11]=[CH:10][N:9]([C:12]2[CH:17]=[CH:16][C:15]([C:18]([F:21])([F:20])[F:19])=[CH:14][CH:13]=2)[N:8]=1)[CH3:5])=[O:3]

Participants

3

Reactant 2

HCID 6329MethylamineHCID 15016300HCID 15016300, compound

Product 1

HCID 15016304HCID 15016304, compound

Procedure

Three g of the product of Example 65 was reacted with 2 ml of aqueous methylamine, substantially as shown in Example 60, to obtain 2.3 g of the desired product, m.p. 157°-158°.

Sources & evidence

ORD record
ord-6bf39f11e9c24a0385e2a27b72b5a94f
Source dataset
uspto-grants-1990_06
Patent number
US04931083

Reaction notes

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