HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-(Piperidin-4-yl)ethyl)piperidine → HCID 14369627, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-(Piperidin-4-yl)ethyl)piperidine | HCID 296292 | — |
| Reactant | 11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one | HCID 11043962 | — |
| Product | HCID 14369627 | HCID 14369627 | 47% |
Reaction Steps
Prepared analogously to Example 4 from 11-(chlorocarbonyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one and 4-[2-(1-piperidinyl)ethyl]piperidine in a yield of 47% of theory. Colourless crystals, m.p. 178°-180° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04931436 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-1c7d160b54e04627a039d3c40c649f46 |
| Source note | uspto-grants-1990_06 |