HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methyl-4,4'-bipiperidine → HCID 14369629, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methyl-4,4'-bipiperidine | HCID 7183041 | — |
| Reactant | 11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one | HCID 11043962 | — |
| Product | HCID 14369629 | HCID 14369629 | 21% |
Reaction Steps
Prepared analogously to Example 4 from 11-(chlorocarbonyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one and 4-(1-methyl-4-piperidinyl)piperidine in a yield of 21% of theory. Colourless crystals, m.p. 254°-255° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04931436 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-25d0446e73eb4fb19a8c1f49125a5f46 |
| Source note | uspto-grants-1990_06 |