HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(2-DIETHYLAMINOETHYL)PIPERIDINE → HCID 14369653, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(2-DIETHYLAMINOETHYL)PIPERIDINE | HCID 296294 | — |
| Reactant | 11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one | HCID 11043962 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 14369653 | HCID 14369653 | 34% |
Reaction Steps
Prepared analogously to Example 4 from 11-(chlorocarbonyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one and 4-[2-(diethylamino)ethyl]piperidine in a yield of 34% of theory. Colourless crystals, m.p. 154° C. (ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04931436 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-d8c796a2ed43470ab3f583569a0ab5a7 |
| Source note | uspto-grants-1990_06 |