HuagongsheHuagongshe Chemistry Print Report · For research reference only
11-(chlorocarbonyl)-6,11-dihydro-5H-pyrido[2,3-b][1,5]benzodiazepin-5-one → HCID 14369668, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 11-(chlorocarbonyl)-6,11-dihydro-5H-pyrido[2,3-b][1,5]benzodiazepin-5-one | HCID 14209983 | — |
| Reactant | HCID 15057323 | HCID 15057323 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14369668 | HCID 14369668 | 72% |
Reaction Steps
Prepared analogously to Example 4 from 11-(chlorocarbonyl)-6,11-dihydro-5H-pyrido[2,3-b][1,5]benzodiazepin-5-one and 4-[4-(1-pyrrolidinyl)butyl]piperidine in a yield of 72% of theory. Colourless crystals, m.p. 193°-195° C. (ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04931436 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-978ac69415d245788ff3ddcd4e059ae4 |
| Source note | uspto-grants-1990_06 |