HuagongsheHuagongshe Chemistry Print Report · For research reference only
11-(chlorocarbonyl)-6,11-dihydro-5H-pyrido[2,3-b][1,5]benzodiazepin-5-one → HCID 23048726, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 11-(chlorocarbonyl)-6,11-dihydro-5H-pyrido[2,3-b][1,5]benzodiazepin-5-one | HCID 14209983 | — |
| Reactant | HCID 15057320 | HCID 15057320 | — |
| Reactant | Hydrate;dihydrochloride | HCID 21226127 | — |
| Product | HCID 23048726 | HCID 23048726 | 48% |
Reaction Steps
Prepared analogously to Example 4 from 11-(chlorocarbonyl)-6,11-dihydro-5H-pyrido[2,3-b][1,5]benzodiazepin-5-one and 2-[2-[[3-(diethylamino)propyl]methylamino]ethyl]piperidine in a yield of 48% of theory. The colourless dihydrochloride-hydrate melted at 145°-150° C. (D.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04931436 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-57d338983ff74752a9ce1305da7eb3f4 |
| Source note | uspto-grants-1990_06 |