HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → 1-(4-Morpholinyl)ethylidene-2-(4-nitrophenyl)hydrazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | 1-(1-Ethoxyethylidene)-2-(4-nitrophenyl)hydrazine | HCID 53940589 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 1-(4-Morpholinyl)ethylidene-2-(4-nitrophenyl)hydrazine | HCID 53687547 | 67% |
Reaction Steps
A mixture of 10 parts of 1-(1-ethoxyethylidene)-2-(4-nitrophenyl)hydrazine, 13 parts of morpholine and 135 parts of methylbenzene was stirred and refluxed for 72 hours. The reaction mixture was cooled. The precipitated product was filtered off, washed with methylbenzene and dried, yielding 8 parts (67%) of 1-[1-(4-morpholinyl)ethylidene]-2-(4-nitrophenyl)hydrazine; mp. 175.9° C. (int. 19)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04931444 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-3856d55577a4449aad01e990479ebb3b |
| Source note | uspto-grants-1990_06 |