HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → Methyl 2-chloro-3-nitrobenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 2-Chloro-3-nitrobenzoic acid | HCID 19870 | — |
| Product | Methyl 2-chloro-3-nitrobenzoate | HCID 10751184 | — |
Reaction Steps
50.0 g (0.248 mol) of 2-chloro-3-nitrobenzoic acid are dissolved in 500 ml of methanol, and 20 ml of concentrated sulfuric acid are added thereto. After refluxing for 24 hours, the mixture is poured onto ice/water and the white precipitate is isolated by filtration, washed with water and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04931581 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-9cae64afbcf243898d60db43c73538cd |
| Source note | uspto-grants-1990_06 |