HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 43449021, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 22403367 | HCID 22403367 | — |
| Product | HCID 43449021 | HCID 43449021 | — |
Reaction Steps
20 ml of concentrated sulfuric acid are added dropwise to 51.0 g (0.182 mol) of 5-bromo-2-chloro-3-nitrobenzoic acid and 500 ml of methanol. The mixture is then boiled under reflux for 16 hours and subsequently cooled with an ice bath and the resulting precipitate is isolated by filtration. The mother liquor is concentrated, water is added and the resulting precipitate is isolated by filtration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04931581 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-ffc5eaa6366d4978ad52247d75d0048f |
| Source note | uspto-grants-1990_06 |