HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54303576, compound → HCID 54183520, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54303576 | HCID 54303576 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 54183520 | HCID 54183520 | — |
Reaction Steps
25.9 g (0.0862 mol) of 3,5-dinitro-2-ethylthiobenzoic acid ethyl ester are dissolved in 260 ml of tetrahydrofuran and hydrogenated at 30°-35° C. in the presence of 10 g of Raney nickel. The catalyst is then isolated by filtration, and the residue is taken up in ethyl acetate, dried over magnesium sulfate, filtered and concentrated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04931581 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-cc648c61fc16444d8bb7d87dc7b53176 |
| Source note | uspto-grants-1990_06 |