HCID 54083756, compound → HCID 54226509, compound

HRID 2106959Notes

Reaction equation

HRID 2106959 reaction equation
[CH3:1][O:2][C:3](=[S:17])[C:4]1[CH:9]=[C:8]([N+:10]([O-])=O)[CH:7]=[C:6]([N+:13]([O-])=O)[C:5]=1[CH3:16]>[Fe]>[CH3:1][O:2][C:3](=[S:17])[C:4]1[CH:9]=[C:8]([NH2:10])[CH:7]=[C:6]([NH2:13])[C:5]=1[CH3:16]

Participants

3

Reactant 1

HCID 54083756HCID 54083756, compound

Product 1

HCID 54226509HCID 54226509, compound

Reagents, catalysts & solvents 1

HCID 23925IronCatalyst

Procedure

Using the method described in Example 1.30, 3,5-dinitro-2-methylthiobenzoic acid methyl ester is reduced using iron turnings to give the title compound which has a melting point of 102°-104° C.

Sources & evidence

ORD record
ord-2922237fa93c4961ad3b3f1423f5c31b
Source dataset
uspto-grants-1990_06
Patent number
US04931581

Reaction notes

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