HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(2-Chloroacetyl)-1,3-dihydro-3-methyl-2H-indol-2-one → HCID 15111515, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(2-Chloroacetyl)-1,3-dihydro-3-methyl-2H-indol-2-one | HCID 4962724 | — |
| Reactant | O-methyl hydrazinecarbothioate | HCID 10171237 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 15111515 | HCID 15111515 | — |
Reaction Steps
1.0 g 5-(2-chloroacetyl)-1,3-dihydro-3-methyl-2H-indol-2-one, 0.37 g O-methyl thiocarbazate, and 20 ml acetonitrile were refluxed for 2 hrs. The precipitate was isolated by filtration and washed with hot acetonitrile to yield a yellowish powder, 450 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933336 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-3e043bc9bf1745018843c558e1c8407d |
| Source note | uspto-grants-1990_06 |