Phenylacetyl chloride → HCID 23047262, compound

Participants

Reaction Steps

Starting from 1,3-dihydro-5(3,6-dihydro-6-methyl-2-oxo-2H-1,3,4-thiadiazin-5-yl)-3,3-dimethyl-2H-indol-2-one (Example 3), this compound was synthesised according to the method described for Example 23 using only one equivalent of potassium hydride and phenylacetyl chloride instead of isonicotinoyl chloride. If an excess of potassium hydride is used in this reaction (2 equivalents) a by-product (described in Example 28) is obtained as the major fraction.

Provenance & Evidence