Hydrogen Bromide → HCID 23047512, compound

HRID 2107071Notes

Reaction equation

HRID 2107071 reaction equation
[C:1]([O-:6])(=[O:5])[C:2]([O-:4])=[O:3].CO[C:9]([C:11]1[CH2:12][NH2+:13][CH2:14][CH:15]([CH3:17])[CH:16]=1)=[O:10].CO[C:20]([C:22]1[CH2:23][NH2+:24][CH2:25][CH:26]([CH3:28])[CH:27]=1)=[O:21].[C:29](=[N:33]O)([NH2:32])[CH2:30][CH3:31].Br.[CH:36]([C:39](=[N:41]O)[NH2:40])(C)[CH3:37]>>[C:1]([O-:6])(=[O:5])[C:2]([O-:4])=[O:3].[CH3:17][CH:15]1[CH2:14][NH2+:13][CH2:12][C:11]([C:9]2[O:10][N:33]=[C:29]([CH2:30][CH3:31])[N:32]=2)=[CH:16]1.[CH3:28][CH:26]1[CH2:25][NH2+:24][CH2:23][C:22]([C:20]2[O:21][N:41]=[C:39]([CH2:36][CH3:37])[N:40]=2)=[CH:27]1

Participants

5

Reactant 4

HCID 260Hydrogen BromideHCID 2794833N'-Hydroxy-2-methylpropanimidamideHCID 4092053N-HydroxypropionimidamideHCID 23047494HCID 23047494, compound

Product 1

HCID 23047512HCID 23047512, compound

Procedure

The compound was synthesized as described in Example 17 using (RS)-3-methoxycarbonyl-5-methyl-1,2,5,6-tetrahydropyridinium oxalate and propionamide oxime instead of arecoline, HBr and isopropylcarboxamide oxime, respectively. M.P. 188°-189° C.

Workup

  1. customThe compound was synthesized

Sources & evidence

ORD record
ord-e0729c71eae748f3a3d15407960bcc47
Source dataset
uspto-grants-1990_06
Patent number
US04933353

Reaction notes

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