HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Thiazolidineacetic acid, 4-oxo-2-thioxo- → HCID 53748478, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Thiazolidineacetic acid, 4-oxo-2-thioxo- | HCID 79793 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | Ethyl 2-(2-Amino-4-thiazolyl)-2-oxoacetate | HCID 4356513 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 53748478 | HCID 53748478 | — |
Reaction Steps
A mixture comprising 4.35 g of ethyl 2-aminothiazol-4-ylglyoxylate, 5 g of rhodanine-3-acetic acid, 2.7 g of sodium acetate and 50 ml of acetic acid was heated under reflux for 2 days. The reaction mixture was then worked up as in Example 1, to give the desired compound as a yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933355 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-6939ba4eb0594c359f88d98f8e939b5e |
| Source note | uspto-grants-1990_06 |