HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 86744020, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | 3-Thiazolidineacetic acid, 4-oxo-2-thioxo- | HCID 79793 | — |
| Reactant | Ethyl 2-(2-Amino-4-thiazolyl)-2-oxoacetate | HCID 4356513 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86744020 | HCID 86744020 | — |
Reaction Steps
The desired compound was prepared by reacting at room temperature, for 15 minutes, 20 g of ethyl 2-aminothiazol-4-ylglyoxylate, 22.9 g of rhodanine-3-acetic acid, 11 g of ammonium chloride, 15 ml of 28% v/v aqueous ammonia and 200 ml of ethanol, following a procedure similar to that described in Example 1. The resulting orange product had the following physical properties.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933355 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-440b614deee142e7b71f71a85ccfa7b1 |
| Source note | uspto-grants-1990_06 |