HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 5-{1-Ethoxycarbonyl-1-[2-(3-phenylureido)thiazol-4-yl]methylene}rhodanine acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | Rhodanine | HCID 1201546 | — |
| Reactant | Ethyl 2-(3-phenylureido)thiazol-4-ylglyoxylate | HCID 15053489 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 5-{1-Ethoxycarbonyl-1-[2-(3-phenylureido)thiazol-4-yl]methylene}rhodanine acetic acid | HCID 54136396 | — |
Reaction Steps
Following a procedure similar to that described in Example 1, the desired compound was prepared from 3 g of ethyl 2-(3-phenylureido)thiazol-4-ylglyoxylate, 1.25 g of rhodanine, 1 g of ammonium chloride 1 ml of 28% v/v aqueous ammonia and 10 ml of ethanol. The resulting product was a yellow powder having the following physical properties.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933355 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-21a70c9232dd45a8ba84d52482b134e2 |
| Source note | uspto-grants-1990_06 |