HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 5-[2-(3-Phenylureido)thiazol-4-ylmethylene]thiazolidine-2,4-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Thiazolidinedione | HCID 5437 | — |
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | 2-(3-Phenylureido)thiazole-4-carbaldehyde | HCID 15053514 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 5-[2-(3-Phenylureido)thiazol-4-ylmethylene]thiazolidine-2,4-dione | HCID 53682958 | — |
Reaction Steps
Following a procedure similar to that described in Example 1, the desired compound was prepared from 1.1 g of 2-(3-phenylureido)thiazole-4-carbaldehyde, 0.52 g of 2,4-thiazolidinedione, 0.6 g of ammonium chloride, 0.6 ml of 28% v/v aqueous ammonia and 20 ml of ethanol. The resulting product was a yellow powder having the following physical properties.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933355 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-4590afc7eebd4b96b64f66fe402339d6 |
| Source note | uspto-grants-1990_06 |