HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 54571816, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | 3-Thiazolidineacetic acid, 4-oxo-2-thioxo- | HCID 79793 | — |
| Reactant | Ethyl 2-(3-p-fluorophenylthioureido)thiazol-4-ylglyoxylate | HCID 15053510 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54571816 | HCID 54571816 | — |
Reaction Steps
Following a procedure similar to that described in Example 1, the desired compound was prepared from 550 mg of ethyl 2-(3-p-fluorophenylthioureido)thiazol-4-ylglyoxylate, 29 mg of rhodanine-3-acetic acid, 150 mg of ammonium chloride, 0.15 ml of 28% v/v aqueous ammonia and 10 ml of ethanol. The resulting product was in the form of yellow acicular crystals having the following physical properties.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933355 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-f3235a84162d4031bb776146a4e10ce3 |
| Source note | uspto-grants-1990_06 |