HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ammonia → 5-(2-Diphenylmethylaminothiazol-4-ylmethylene)rhodanine--acetic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ammonia | HCID 222 | — |
| Edukt | Ammonium Chloride | HCID 25517 | — |
| Edukt | 3-Thiazolidineacetic acid, 4-oxo-2-thioxo- | HCID 79793 | — |
| Edukt | 2-Diphenylmethylaminothiazole-4-carbaldehyde | HCID 23047635 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 5-(2-Diphenylmethylaminothiazol-4-ylmethylene)rhodanine--acetic acid | HCID 54571765 | — |
Reaktionsschritte
Following a procedure similar to that described in Example 1, the desired compound was prepared from 1.95 g of 2-diphenylmethylaminothiazole-4-carbaldehyde. 1.32 g of rhodanine-3-acetic acid, 0.4 g of ammonium chloride, 0.4 ml of 28% v/v aqueous ammonia and 20 ml of ethanol. The resulting product was a reddish-brown powder having the following physical properties.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04933355 |
| Quelldatensatz | uspto-grants-1990_06 |
| ORD ID | ord-32d7fa8a3a684f44be86cf99725fada2 |
| Quellennotiz | uspto-grants-1990_06 |