1-Isocyanato-4-methoxybenzene → HCID 15053492, compound

HRID 2107225Notes

Reaction equation

HRID 2107225 reaction equation
[NH2:1][C:2]1[S:3][CH:4]=[C:5]([C:7](=[O:13])[C:8]([O:10][CH2:11][CH3:12])=[O:9])[N:6]=1.[CH3:14][O:15][C:16]1[CH:21]=[CH:20][C:19]([N:22]=[C:23]=[O:24])=[CH:18][CH:17]=1>CN(C)C=O>[CH3:14][O:15][C:16]1[CH:21]=[CH:20][C:19]([NH:22][C:23](=[O:24])[NH:1][C:2]2[S:3][CH:4]=[C:5]([C:7](=[O:13])[C:8]([O:10][CH2:11][CH3:12])=[O:9])[N:6]=2)=[CH:18][CH:17]=1

Participants

4

Reactant 2

HCID 794431-Isocyanato-4-methoxybenzeneHCID 4356513Ethyl 2-(2-Amino-4-thiazolyl)-2-oxoacetate

Product 1

HCID 15053492HCID 15053492, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

Following the procedures in preparation 1, the desired compound was prepared using 10 g of ethyl 2-aminothiazol-4-ylglyoxylate, 9 g of p-methoxyphenyl isocyanate and 80 ml of dimethylformamide as yellow powders. The product has the following physical properties.

Workup

  1. customin preparation 1

Sources & evidence

ORD record
ord-f16bdddb22aa46129dbc2a76f71505aa
Source dataset
uspto-grants-1990_06
Patent number
US04933355

Reaction notes

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