HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Xylyl isocyanate → Ethyl 2-[3-(2,6-xylyl)ureido]thiazol-4-ylglyoxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Xylyl isocyanate | HCID 98787 | — |
| Reactant | Ethyl 2-(2-Amino-4-thiazolyl)-2-oxoacetate | HCID 4356513 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Ethyl 2-[3-(2,6-xylyl)ureido]thiazol-4-ylglyoxylate | HCID 15053505 | — |
Reaction Steps
Following a procedure similar to that described in Preparation 1, the desired compound was prepared from 5 g of ethyl 2-aminothiazol-4-ylglyoxylate, 5.5 g of 2,6-xylyl isocyanate and 30 ml of dimethylformamide. The resulting product was a pale yellow powder having the following physical properties.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933355 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-b75385a1c230444bb9c16139a3165f3b |
| Source note | uspto-grants-1990_06 |