HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → Ethyl 2-(diethylamino)-1,3-thiazole-4-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethyl 2-chlorothiazole-4-carboxylate | HCID 13106141 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Ethyl 2-(diethylamino)-1,3-thiazole-4-carboxylate | HCID 12966399 | — |
Reaction Steps
The reaction described in Preparation 26 was repeated, but using 2.3 g of diethylamine, 4 g of ethyl 2-chlorothiazole-4-carboxylate, 4.2 g of triethylamine, and 15 ml of dimethylformamide, giving ethyl 2-diethylaminothiazole-4-carboxylate as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933355 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-b3702451474c4f5f89fa7fae49e286ae |
| Source note | uspto-grants-1990_06 |