HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluorophenyl isothiocyanate → HCID 15053509, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluorophenyl isothiocyanate | HCID 97520 | — |
| Reactant | Ethyl 2-(2-Amino-4-thiazolyl)-2-oxoacetate | HCID 4356513 | — |
| Solvent | Hexamethylphosphoramide | HCID 12679 | — |
| Product | HCID 15053509 | HCID 15053509 | — |
Reaction Steps
Following a procedure similar to that described in Preparation 1. the desired compound was prepared from 15 g of ethyl 2-aminothiazol-4-ylglyoxylate, 17 g of o-fluorophenyl isothiocyanate and 30 ml of hexamethylphosphoric triamide. The resulting product was a pale yellow powder having the following physical properties.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933355 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-70e4fd2e0e5b4b8dbd1fcbd16579eb02 |
| Source note | uspto-grants-1990_06 |