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HRID2107260

反应详情

EQUATION

反应方程式

HRID 2107260 的结构方程式

REACTANTS

反应物

2
结构：CCOC(=O)c1csc(Nc2ccccc2)n1
HCID15053537

Ethyl 2-anilino-1,3-thiazole-4-carboxylate

C12H12N2O2S

结构：[Al+3].[H-].[H-].[H-].[H-].[Li+]
HCID21226445

未命名化合物

PRODUCTS

生成物

1
结构：OCc1csc(Nc2ccccc2)n1
HCID15053553

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

Following a procedure similar to that described in Preparation 15, the desired compound was prepared from 8.5 g of ethyl 2-anilinothiazol-4-carboxylate, 2 g of lithium aluminum hydride and 150 ml of tetrahydrofuran, as colorless flakes having the following physical properties.

WORKUP

后处理

  1. customthat described in Preparation 15